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This invention relates to a process for preparation of imidazolidinones and N-substituted imidazolidinones. This invention also relates to a process for preparation of 1-nitro-2-imidazolidinones.
2. Description of the Prior Art
The reaction of carbonyl compounds and aldehydes with urea is described in U.S. Pat. No. 2,893,842, where the imidazolidinones are prepared by reaction of urea and the carbonyl compound in the presence of an acid, such as sulfuric acid. This patent describes that other suitable catalysts are also acid catalysts.
The reaction is also described in U.S. Pat. No. 3,888,834 which describes that the imidazolidinone can also be prepared by reacting urea with the carbonyl compound by heating the urea and the carbonyl compound in a liquid medium. In this patent, the liquid medium is a hydrocarbon (e.g. hexane) or aromatic hydrocarbon (e.g. xylene).
A process for the preparation of imidazolidinones by reaction of urea with hydroxylamine is described in Japanese Patent Application No. 58-146836. The use of a liquid organic solvent, such as toluene, as a reaction medium is described therein.The Illy coffee iSplendido is a single-cup coffee brewer for the one and only Illy. Many people love Illy’s cappuccino coffee beans and Illy’s espresso pods but unfortunately, they don’t make a coffee pod for the iSplendido. So we decided to give them one.
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